X PERT HIGHSCORE PLUS SOFTWARE GENERATOR
X PERT HIGHSCORE PLUS SOFTWARE PRO
X PERT HIGHSCORE PLUS SOFTWARE SOFTWARE

Axios can be used to measure SMALL samples, but having one dimension at least 6mm. The time of measurement was about 20 min. The analysed powders were pressed into pellets about 5mm thick and diameter of 40 mm without any binding agent (or with Dentakryl as binding agent if F,O,N,C,B elements must be measured or sample does not stick together by pressing) and covered with 4 μm supporting polypropylene (PP) film.

X PERT HIGHSCORE PLUS SOFTWARE SOFTWARE

The obtained data were evaluated by standardless software Omnian.

X PERT HIGHSCORE PLUS SOFTWARE GENERATOR

The generator settings-collimator-crystal-detector combinations were optimized for collecting 11 scans for all 83 measured elements, for a lot of elements are more than one X-ray line available. All peak intensity data were collected by software SuperQ 5.0 in vacuum. It is equipped with a Rh anode end-window X-ray tube type 4GN fitted with 75 μm Be window. The time of measurement was about 15 min.Īn Axios sequential WD-XRF spectrometer was used to perform XRF analysis. The analyzed powders were pressed into pellets about 5mm thick and diameter of 40 mm without any binding agent (or with Dentakryl as binding agent if F,O,N,C,B elements must be measured or sample does not stick together by pressing) and covered with 4 μm supporting polypropylene (PP) film. The obtained data were evaluated by standardless software Uniquant 4. The generator settings-collimator-crystal-detector combinations were optimised for all 82 measured elements with analysis time of 6s per element.

All peak intensity data were collected by software WinXRF in vacuum. It is equipped with a Rh anode end-window X-ray tube type 4GN fitted with 50 μm Be window. WD-XRF analysisĪn ARL 9400 XP sequential WD-XRF spectrometer was used to perform XRF analysis. Debye-Scherrer frames were converted into a standard 1D powder pattern in the software package Bruker EVA 4.0. Two images (Debye-Scherrer frames) were collected in θ-θ geometry for 2θ = 26°, 56° with 2D detector Vantech and counting time of 30min per image. X-ray powder diffraction data from microspot were collected at room temperature with an D8 Discover microdiffraction system with parallel geometry using CoK α radiation (λ = 1.7903 Å, U = 35 kV, I = 40 mA). The maximum weight of the sample is 2 kg, height 50mm. Sample is placed on XYZ programmable stage with X,Y,Z translations in range 0-25mm. MicroXRD – microdiffraction system D8 Discover with 2D Vantech detector The sample was heated and cooled with rate 10 ☌/min. The heating and cooling process was controlled by Eurotherm 2404. Data were scanned with an ultrafast detector Lyn圎ye over the angular range 3-38° (2θ) with a step size of 0.0196° (2θ) and a counting time of 58.6 s step -1. The sample was placed on a Pt/Rh ribbon in a MRI high-temperature oven-camera and VPSlits were used to fix the constant irradiated length (20 mm). Temperature dependent X-ray powder diffraction (TDXD) was carried out with a Bruker AXS D8 θ-θ powder diffractometer with parafocusing Bragg-Brentano geometry using CoK α radiation (λ = 1.79028 Å, U = 34 kV, I = 30 mA). High temperature X-ray diffraction analysis Data evaluation was performed in the software package HighScore Plus 4.0. Data were scanned with an ultrafast detector 1D detector PIXCEL over the angular range 5-60° (2θ) with a step size of 0.013° (2θ) and a counting time of 56.86 s step -1. X-ray powder diffraction data were collected at room temperature with an X'Pert 3 Powder θ-θ powder diffractometer with parafocusing Bragg-Brentano geometry using CuK α radiation (λ = 1.5418 Å, U = 40 kV, I = 30 mA). Data were scanned with an ultrafast detector X'Celerator (or with a scintilator detector equipped with a secondary curved monochromator) over the angular range 5-60° (2θ) with a step size of 0.017° (2θ) and a counting time of 20.32 s step -1.

X PERT HIGHSCORE PLUS SOFTWARE PRO

X-ray powder diffraction data were collected at room temperature with an X'Pert PRO θ-θ powder diffractometer with parafocusing Bragg-Brentano geometry using CoK α radiation (λ = 1.79028 Å, U = 35 kV, I = 40 mA). Data evaluationwere performed in the software package HighScore Plus 4.0. Data were scanned with an ultrafast detector Lyn圎ye over the angular range 5-60° (2θ) with a step size of 0.0196° (2θ) and a counting time of 19.2 s step -1. X-ray powder diffraction data were collected at room temperature with a Bruker AXS D8 θ-θ powder diffractometer with parafocusing Bragg-Brentano geometry using CoK α radiation (λ = 1.79028 Å, U = 34 kV, I = 20 or 30 mA). XRD and XRF data collection Ambient temperature X-ray diffraction analysis

X Pert Highscore Plus Software